▒ (1-x)Pb(Zr0.52Ti0.48)O3.- x(Bi3.25La0.75)Ti3O12 (when x = 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1.0)의 참조표준  
참조표준 번호 KSRD.01.2008.001.033
참조표준 등급 유효 참조표준
Composition Density
(g cm-3)
Dielectric propertiesε ra Dielectric propertiesε
tanδ
Ferroelectric properties
Pr/Pmax
Ferroelectric properties
Ec/Emax
Loop
squareness(Rsq)
PZT 7.61 1011 0.014 0.43 0.29 1.14
0.9PZT-0.1BLT 7.68 896 0.055 0.66 0.55 1.58
0.7PZT-0.3BLT 7.53 303 0.012 - - -
0.5PZT-0.5BLT 7.37 328 0.016 - - -
0.3PZT-0.7BLT 7.49 330 0.022 - - -
0.1PZT-0.9BLT 7.56 304 0.016 - - -
BLT 7.44 145 0.01 - - -
측정불확도 측정불확도: 전기기계 결합계수(kp),(측정장비 : HP 4194A) : 0.02259
▒ (1-x)Pb(Zr0.52Ti0.48)O3.- x(Bi3.25La0.75)Ti3O12 (when x = 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1.0)의 참조표준 기본정보  
재료규격 조성: (1-x)Pb(Zr0.52Ti0.48)O3.- x(Bi3.25La0.75)Ti3O12 (when x = 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1.0)
원료순도: PbO(99%), ZrO2(99%), TiO2(99%), Bi2O3(98%), La2CO3(99%)
혼합 및 분쇄: 볼밀 24h,
하소/소결: 750℃ 4h(BLT), 800℃ 2h(PZT)/1150℃ 4h
전극: Silver paste
결정구조/소결특성
측정방법 측정/장비: XRD (Phillp Model X-pert), 유전측정기 (Hewlett-Packard 4194A)
시편형상: Disk
▒ (1-x)Pb(Zr0.52Ti0.48)O3.- x(Bi3.25La0.75)Ti3O12 (when x = 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1.0)의 참조표준 문서자료  
  • [저널정보] Current Applied Physics / Structure-property relation of ferroelectric Pb(Zr0.52Ti0.48)O3-(Bi3.25La0.75)TiO12 ceramics / 8 / / 367-371 ( 2008)


▒ 0.9Pb(Zr0.52Ti0.48)O3.- 0.1Pb(Mg1/3Nb2/3)O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.032
참조표준 등급 유효 참조표준
Sintering
temperature(℃)
Grain size(μm) Pr(μC/cm2) Ps(μC/cm2) Ec(kV/cm) εr d31
1150 2 0.38 0.79 1.25 1020 95
1200 3.5 0.86 1.52 1.53 1150 110
1250 5 1.62 3.26 0.68 1400 160
1300 9 1.21 2.42 1.72 1370 130
0.3PZT-0.7BLT 7.49 330 0.022 - - -
0.1PZT-0.9BLT 7.56 304 0.016 - - -
BLT 7.44 145 0.01 - - -
측정불확도 측정불확도: 전기기계 결합계수(kp),(측정장비 : HP 4294A) : 0.02259
▒ 0.9Pb(Zr0.52Ti0.48)O3.- 0.1Pb(Mg1/3Nb2/3)O3의 참조표준 기본정보  
재료규격 조성: 0.9Pb(Zr0.52Ti0.48)O3.- 0.1Pb(Mg1/3Nb2/3)O3.
원료순도: PbO, ZrO2, TiO2, MgO and Nb2O5 (were supplied from Shenzhen Yujie Co., China)
혼합 및 분쇄: 습슥혼합, 볼밀
하소/소결: 850℃ 2h/1100℃-1300℃ 2h
전극: Silver paste
결정구조/소결특성/기본물성: XRD/ SEM/εr, kp, d33, Ec,
측정방법 측정/장비: Impedance analyzer (HP4294A)
시편형상: Disk
▒ 0.9Pb(Zr0.52Ti0.48)O3.- 0.1Pb(Mg1/3Nb2/3)O3의 참조표준 문서자료  
  • [저널정보] Journal of Alloys and Compounds / The influence of sintering conditions on the dielectric and piezoelectric properties of PbZrTiO-PbMgNbo ceramic tubes / / / ( 2008)


▒ Pb1-0.5x(Zr0.52Ti0.48)1-xNbxO3 (x = 0.02-0.06)의 참조표준  
참조표준 번호 KSRD.01.2008.001.031
참조표준 등급 유효 참조표준
Compositions Density
(g/cm3)
Kp εr Reference Poling Field Kt Kt Kt Kt Kt Kp Kp Kp Kp Kp Dielectric
Constant
Dielectric
Constant
Dielectric
Constant
Dielectric
Constant
Dielectric
Constant
Loss
factor
Loss
factor
Loss
factor
Loss
factor
Loss
factor
Pure PZT(52/48) 7.4 0.47 707 [3] x=0.02 x=0.04 x=0.05 x=0.055 x=0.06 x=0.02 x=0.04 x=0.05 x=0.055 x=0.06 x=0.02 x=0.04 x=0.05 x=0.055 x=0.06 x=0.02 x=0.04 x=0.05 x=0.055 x=0.06
PZT: Sr 7.1 0.44 973 [3] 0 0 0 0 0 0 0 0 0 0 0 1050 900 900 1150 1050 2.5 3 2.7 3.5 2.8
PZT: Sr 7.5 0.52 1300 [1] 5 0.25 0.3 0.22 0.2 25 0.25 0.2 0.25 0.32 0.3 1100 950 1100 1350 1100 2.2 2.5 2.5 2.2 2.2
PZT: Ca 7.42 0.49 729 [3] 10 0.35 0.4 0.38 0.38 0.32 0.45 0.48 0.5 0.5 0.48 1200 1100 1250 1400 1250 1.8 2.2 1.8 2 2
PZT: Y 7.26 0.34 841 [4] 20 0.45 0.42 0.4 0.42 0.4 0.5 0.5 0.52 0.57 0.5 1200 1100 1300 1450 1300 1.8 2.2 1.8 1.9 1.8
PZT: La 7.46 0.53 1483 [4] 30 0.4 0.42 0.5 0.51 0.48 0.5 0.52 0.53 0.6 0.5 1150 1100 1300 1500 1300 1.7 1.8 1.6 1.8 1.9
PZT: Nb 7.43 0.49 1395 [4] 40 0.46 0.4 0.48 0.46 0.46 0.5 0.52 0.53 0.58 0.52 1050 1050 1300 1450 1300 1.6 1.7 1.5 1.8 1.9
PZT: (Nb+Sr) 7.35 0.49 1776 [4] 50 0.46 0.4 0.48 0.42 0.42 0.5 0.52 0.53 0.6 0.52 1050 1050 1300 1400 1300 1.5 1.6 1.5 1.7 1.8
PZT: Nb 7.6 0.54 1242 [4]
PZT:(La+Nb) 7.39 0.57 1377 [4]
PZT: Ta 7.49 0.5 1230 [4]
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
▒ Pb1-0.5x(Zr0.52Ti0.48)1-xNbxO3 (x = 0.02-0.06)의 참조표준 기본정보  
재료규격 조성: Pb1-0.5x(Zr0.52Ti0.48)1-xNbxO3 (x = 0.02-0.06)
원료순도: PbO(>99%), ZrO2(>99%), TiO2(>99%), Nb2O5(>99%)
혼합 및 분쇄: 볼밀 4시간, 미디어 ZrO2
하소/성형/소결: 900℃ 3시간/1축 press 25Kg/cm2 /1250℃, 2시간
전극: Silver paste
결정구조/소결특성/기본물성: XRD/ SEM/ εr, tan δ, kp,
측정방법 측정/장비: Impedance analyzer (HP4294A)
시편형상: Disk, 직경 12mm, 두께 1mm
▒ Pb1-0.5x(Zr0.52Ti0.48)1-xNbxO3 (x = 0.02-0.06)의 참조표준 문서자료  
  • [저널정보] / Effects of poling field on the piezoelectric and dielectric properties of Nb additive PZT-based ceramics and their applications on SAW devices / / / ( )


▒ 0.90Pb0.95Sr0.05(Pb (Zr0.52Ti0.48)O3 + x wt % WO3,Y2O3,MoO3의 참조표준  
참조표준 번호 KSRD.01.2008.001.030
참조표준 등급 유효 참조표준
Sample ε33(unpoled) ε33T(poled) Kp Kt
PZT 911 938 0.48 0.43
0.1wt.%Y2O3 1006 992 0.5 0.4
0.5wt.%Y2O3 985 954 0.3 0.27
1.0wt.%Y2O3 913 878 0.23 0.14
0.5wt.%MoO3 977 964 0.43 0.47
1.0wt.%MoO3 961 937 0.42 0.4
0.1wt.%MoO3 792 724 0.29 0.3
0.1wt.%WO3 933 858 0.47 0.43
0.5wt.%WO3 1038 979 0.42 0.39
1.0wt.%WO3 1281 1170 0.38 0.29
973 [3] 0 0 0 0 0 0 0 0 0 0 0 1050 900 900 1150 1050 2.5 3 2.7 3.5 2.8
PZT: Sr 7.5 0.52 1300 [1] 5 0.25 0.3 0.22 0.2 25 0.25 0.2 0.25 0.32 0.3 1100 950 1100 1350 1100 2.2 2.5 2.5 2.2 2.2
PZT: Ca 7.42 0.49 729 [3] 10 0.35 0.4 0.38 0.38 0.32 0.45 0.48 0.5 0.5 0.48 1200 1100 1250 1400 1250 1.8 2.2 1.8 2 2
PZT: Y 7.26 0.34 841 [4] 20 0.45 0.42 0.4 0.42 0.4 0.5 0.5 0.52 0.57 0.5 1200 1100 1300 1450 1300 1.8 2.2 1.8 1.9 1.8
PZT: La 7.46 0.53 1483 [4] 30 0.4 0.42 0.5 0.51 0.48 0.5 0.52 0.53 0.6 0.5 1150 1100 1300 1500 1300 1.7 1.8 1.6 1.8 1.9
PZT: Nb 7.43 0.49 1395 [4] 40 0.46 0.4 0.48 0.46 0.46 0.5 0.52 0.53 0.58 0.52 1050 1050 1300 1450 1300 1.6 1.7 1.5 1.8 1.9
PZT: (Nb+Sr) 7.35 0.49 1776 [4] 50 0.46 0.4 0.48 0.42 0.42 0.5 0.52 0.53 0.6 0.52 1050 1050 1300 1400 1300 1.5 1.6 1.5 1.7 1.8
PZT: Nb 7.6 0.54 1242 [4]
PZT:(La+Nb) 7.39 0.57 1377 [4]
PZT: Ta 7.49 0.5 1230 [4]
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
▒ 0.90Pb0.95Sr0.05(Pb (Zr0.52Ti0.48)O3 + x wt % WO3,Y2O3,MoO3의 참조표준 기본정보  
재료규격 조성: Pb (Zr0.52Ti0.48)O3 + x wt % WO3,Y2O3,MoO3
원료순도: 제시하지않음
혼합 및 분쇄: 볼밀 6시간, 미디어 iron
하소/성형/소결: 850℃ 2시간/1축 press, 1260℃, 1.5시간
전극: Silver paste
결정구조/소결특성/기본물성: XRD/ SEM/ density (g/㎤), εr, kp, 파괴강도, 파괴인성
측정방법 측정/장비: 미세구조 (Field Emission Scanning Electron Microscopy) Impedance analyzer (HP4294A)
시편형상: Disk, 직경 17mm, 두께 2mm / Rectangle body, 직경 42mm, 두께 8mm
▒ 0.90Pb0.95Sr0.05(Pb (Zr0.52Ti0.48)O3 + x wt % WO3,Y2O3,MoO3의 참조표준 문서자료  
  • [저널정보] Ceramics International / Mechanical and electrical properties of small amount of oxides reinforced PZT ceramics / 29 / / 499-503 ( 2003)


▒ Pb(Zr0.475Ti0.525)O3?Pb(Mg1/3Nb2/3)O3?Pb(Fe1/2Nb1/2)O3 + Li2CO3의 참조표준  
참조표준 번호 KSRD.01.2008.001.029
참조표준 등급 유효 참조표준
Composition
(milling method)
Ts(℃) Sintered density
(g/cm3)
Average grain
size(μm)
kp d33(pC/N) Hv(kgf/mm2) KIC(Mpa m1/2)
PZT ceramics(CBM) 1200 7.72 5.4 0.39 243 418 1.2
PFMNZT(CBM) 950 7.95 3.3 0.67 575 437 0.69
900 7.96 3 0.64 521 443 0.64
850 7.81 1.8 0.61 490 418 0.74
PFMNZT(HEBM) 950 7.97 3.1 0.68 594 454 0.65
900 7.99 2.2 0.67 563 458 0.76
850 8.01 1.7 0.64 511 469 0.67
0 0 0 0 1050 900 900 1150 1050 2.5 3 2.7 3.5 2.8
PZT: Sr 7.5 0.52 1300 [1] 5 0.25 0.3 0.22 0.2 25 0.25 0.2 0.25 0.32 0.3 1100 950 1100 1350 1100 2.2 2.5 2.5 2.2 2.2
PZT: Ca 7.42 0.49 729 [3] 10 0.35 0.4 0.38 0.38 0.32 0.45 0.48 0.5 0.5 0.48 1200 1100 1250 1400 1250 1.8 2.2 1.8 2 2
PZT: Y 7.26 0.34 841 [4] 20 0.45 0.42 0.4 0.42 0.4 0.5 0.5 0.52 0.57 0.5 1200 1100 1300 1450 1300 1.8 2.2 1.8 1.9 1.8
PZT: La 7.46 0.53 1483 [4] 30 0.4 0.42 0.5 0.51 0.48 0.5 0.52 0.53 0.6 0.5 1150 1100 1300 1500 1300 1.7 1.8 1.6 1.8 1.9
PZT: Nb 7.43 0.49 1395 [4] 40 0.46 0.4 0.48 0.46 0.46 0.5 0.52 0.53 0.58 0.52 1050 1050 1300 1450 1300 1.6 1.7 1.5 1.8 1.9
PZT: (Nb+Sr) 7.35 0.49 1776 [4] 50 0.46 0.4 0.48 0.42 0.42 0.5 0.52 0.53 0.6 0.52 1050 1050 1300 1400 1300 1.5 1.6 1.5 1.7 1.8
PZT: Nb 7.6 0.54 1242 [4]
PZT:(La+Nb) 7.39 0.57 1377 [4]
PZT: Ta 7.49 0.5 1230 [4]
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4194A) : 0.02259
▒ Pb(Zr0.475Ti0.525)O3?Pb(Mg1/3Nb2/3)O3?Pb(Fe1/2Nb1/2)O3 + Li2CO3의 참조표준 기본정보  
재료규격 조성: Pb(Zr0.475Ti0.525)O3?Pb(Mg1/3Nb2/3)O3?Pb(Fe1/2Nb1/2)O3 + Li2CO3
원료순도: 제시하지않음
혼합 및 분쇄: columbite precursor 방법
하소/성형/소결: 1050℃ 4시간/1축 press, 850℃-950℃, 2시간
전극: Silver paste
소결특성/기본물성: SEM/ density (g/㎤), kp, d33,Hardness, fracture toughness
측정방법 측정/장비: impedance analyzer (HP4194A)
시편형상: Disk, 직경 18mm, 두께 0.8mm
측정환경: 20oC, 1kHz
▒ Pb(Zr0.475Ti0.525)O3?Pb(Mg1/3Nb2/3)O3?Pb(Fe1/2Nb1/2)O3 + Li2CO3의 참조표준 문서자료  
  • [저널정보] Ceramics International / Effects of high energy ball-milling on the sintering behavior and piezoelectric properties of PZT-based ceramics / 33 / / 1283-1286 ( 2007)


▒ 0.90Pb0.95Sr0.05(Zr0.52Ti0.48)O3 - 0.03Pb(Fe2/3 W1/3)O3 - 0.07Pb(Mn1/3Nb2/3)O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.028
참조표준 등급 유효 참조표준
Sample Kp Qm d33
(ρC/N)
εr tanδ
x=0 wt% WO3 0.64 1750 370 1730 0.0057
x=0.05 wt% WO3 0.65 1800 365 1800 0.005
x=0.1 wt% WO3 0.65 1870 355 1790 0.0052
x=0.15 wt% WO3 0.64 1880 350 1800 0.0052
x=0.2 wt% WO3 0.64 1920 340 1840 0.0054
x=0.25 wt% WO3 0.64 1600 370 1880 0.0059
x=0.3 wt% WO3 0.64 1550 400 1900 0.006
900 7.99 2.2 0.67 563 458 0.76
850 8.01 1.7 0.64 511 469 0.67
0 0 0 0 1050 900 900 1150 1050 2.5 3 2.7 3.5 2.8
PZT: Sr 7.5 0.52 1300 [1] 5 0.25 0.3 0.22 0.2 25 0.25 0.2 0.25 0.32 0.3 1100 950 1100 1350 1100 2.2 2.5 2.5 2.2 2.2
PZT: Ca 7.42 0.49 729 [3] 10 0.35 0.4 0.38 0.38 0.32 0.45 0.48 0.5 0.5 0.48 1200 1100 1250 1400 1250 1.8 2.2 1.8 2 2
PZT: Y 7.26 0.34 841 [4] 20 0.45 0.42 0.4 0.42 0.4 0.5 0.5 0.52 0.57 0.5 1200 1100 1300 1450 1300 1.8 2.2 1.8 1.9 1.8
PZT: La 7.46 0.53 1483 [4] 30 0.4 0.42 0.5 0.51 0.48 0.5 0.52 0.53 0.6 0.5 1150 1100 1300 1500 1300 1.7 1.8 1.6 1.8 1.9
PZT: Nb 7.43 0.49 1395 [4] 40 0.46 0.4 0.48 0.46 0.46 0.5 0.52 0.53 0.58 0.52 1050 1050 1300 1450 1300 1.6 1.7 1.5 1.8 1.9
PZT: (Nb+Sr) 7.35 0.49 1776 [4] 50 0.46 0.4 0.48 0.42 0.42 0.5 0.52 0.53 0.6 0.52 1050 1050 1300 1400 1300 1.5 1.6 1.5 1.7 1.8
PZT: Nb 7.6 0.54 1242 [4]
PZT:(La+Nb) 7.39 0.57 1377 [4]
PZT: Ta 7.49 0.5 1230 [4]
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp)의,(측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33),(측정장비 : ZJ-3d) : 0.5(pC/N)
▒ 0.90Pb0.95Sr0.05(Zr0.52Ti0.48)O3 - 0.03Pb(Fe2/3 W1/3)O3 - 0.07Pb(Mn1/3Nb2/3)O3의 참조표준 기본정보  
재료규격 조성: 0.90Pb0.95Sr0.05(Zr0.52Ti0.48)O3-0.03Pb(Fe2/3 W1/3)O3-0.07Pb(Mn1/3Nb2/3)O3 + 0.2wt.%CeO2 + xwt.%Pb3O4 (x = 0.0, 0.5, 1.0, 2.0, 2.5, 3.0, 4.0, 5.0) + ywt.%WO3 (y = 0.00, 0.05, 0.10, 0.15, 0.20, 0.25, 0.30)
시편형상 및 제조방법: disk type, 직경 15mm
원료: Pb3O4(97%)
측정방법 측정/장비: XRD/(XRD Model DMX-2550/PC, Rigaku, Japa), SEM/(Quanta200, FEI Compan), LCR meter, impedance analyzer/(HP Model 4294A),quasi-static piezoelectric d33 meter/(Model ZJ-3d, Institute of Acoustics Academic
Sinica, China)
시편형상 : 직경 15mm
측정환경:
▒ 0.90Pb0.95Sr0.05(Zr0.52Ti0.48)O3 - 0.03Pb(Fe2/3 W1/3)O3 - 0.07Pb(Mn1/3Nb2/3)O3의 참조표준 문서자료  
  • [저널정보] Materials Research Bulletin / Effects of WO3 addition on the structure and electrical properties of Pb3O4 modified PZT-PFW-PMN piezoelectric ceramics / 41 / / 1447-1454 ( 2006)

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▒ (1-x)PbNb2O6.- xCa0.6TiO3의 참조표준  
참조표준 번호 KSRD.01.2008.001.027
참조표준 등급 유효 참조표준
Tc (℃) d33
(ρC/N)
Kt Kp Kt/Kp Qm εT330 tan δ Nφ (㎐ m)
PN 530 221
PNT1 565 81 0.374 0.116 3.22 26.9 244 0.0097 1835
PNT2 582 76 0.386 0.104 3.71 24 263 0.014 1850
PNT3 604 72 0.362 0.089 4.07 23.5 286 0.015 1854
PNT4 612 69 0.331 0.094 3.52 19.6 294 0.012 1863
0.64 511 469 0.67
0 0 0 0 1050 900 900 1150 1050 2.5 3 2.7 3.5 2.8
PZT: Sr 7.5 0.52 1300 [1] 5 0.25 0.3 0.22 0.2 25 0.25 0.2 0.25 0.32 0.3 1100 950 1100 1350 1100 2.2 2.5 2.5 2.2 2.2
PZT: Ca 7.42 0.49 729 [3] 10 0.35 0.4 0.38 0.38 0.32 0.45 0.48 0.5 0.5 0.48 1200 1100 1250 1400 1250 1.8 2.2 1.8 2 2
PZT: Y 7.26 0.34 841 [4] 20 0.45 0.42 0.4 0.42 0.4 0.5 0.5 0.52 0.57 0.5 1200 1100 1300 1450 1300 1.8 2.2 1.8 1.9 1.8
PZT: La 7.46 0.53 1483 [4] 30 0.4 0.42 0.5 0.51 0.48 0.5 0.52 0.53 0.6 0.5 1150 1100 1300 1500 1300 1.7 1.8 1.6 1.8 1.9
PZT: Nb 7.43 0.49 1395 [4] 40 0.46 0.4 0.48 0.46 0.46 0.5 0.52 0.53 0.58 0.52 1050 1050 1300 1450 1300 1.6 1.7 1.5 1.8 1.9
PZT: (Nb+Sr) 7.35 0.49 1776 [4] 50 0.46 0.4 0.48 0.42 0.42 0.5 0.52 0.53 0.6 0.52 1050 1050 1300 1400 1300 1.5 1.6 1.5 1.7 1.8
PZT: Nb 7.6 0.54 1242 [4]
PZT:(La+Nb) 7.39 0.57 1377 [4]
PZT: Ta 7.49 0.5 1230 [4]
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp),(측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33), (측정장비 : ZJ-3d) : 0.5(pC/N)
▒ (1-x)PbNb2O6.- xCa0.6TiO3의 참조표준 기본정보  
재료규격 조성: (1-x)PbNb2O6.- xCa0.6TiO3 (x=0,0.01, 0.02, 0.03, and 0.04 mol),
시편형상 및 제조방법: disk type, 직경:20mm, 두께:1.5mm
원료순도: Reagent grade oxide, PbO, TiO2, Nb2O55%), CaCO3
혼합 및 분쇄: planetary milling, alcohol, 10시간.
하소/성형/소결: 850℃4h /150MPa/1240℃-1260℃ 4h
전극/분극: S
측정방법 측정/장비: TH2828 LRC meter, quasistatic d33 meter (ZJ-3A), impedance analyzer (HP4294A), Radiant Precision Workstation ferroelectric testing system
시편형상: .15mm×1mm disks
측정환경: 상온~620℃
▒ (1-x)PbNb2O6.- xCa0.6TiO3의 참조표준 문서자료  
  • [저널정보] journal of materials processing technology / Piezoelectric and dielectric properties of PbNb2O6-based piezoelectric ceramics with high Curie temperature / 197 / / 170-173 ( 2008)

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▒ 0.05Pb(Mg1/3Nb2/3)O3 -0.05Pb(Zn1/3Nb2/3)O3 -0.90Pb (Zr0.52-Ti0.48)O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.026
참조표준 등급 유효 참조표준
Sintering
temperature (℃)
Calcination
temperature (℃)
d33
(ρC/N)
Kp Qm tan δ εr
980 700 225 0.54 1351 0.0069 1031
750 229 0.55 1467 0.0067 1041
780 231 0.55 1467 0.0066 1056
800 237 0.55 1632 0.0062 1089
820 233 0.54 1508 0.0069 1079
850 232 0.53 1508 0.007 1055
880 227 0.52 976 0.0074 1027
1000 700 231 0.55 1108 0.0069 1040
750 237 0.55 1336 0.0067 1059
780 237 0.55 1562 0.0066 1078
800 241 0.56 1637 0.0063 1102
820 238 0.56 1584 0.0066 1093
850 236 0.55 1535 0.0067 1088
880 228 0.54 1145 0.0068 1055
1020 700 234 0.55 1158 0.0069 1061
750 238 0.56 1736 0.0068 1095
780 244 0.57 1795 0.0064 1095
800 249 0.57 1954 0.0059 1122
820 242 0.57 1822 0.0061 1111
850 236 0.56 1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33), (측정장비 : ZJ-3d) : 0.5(pC/N)
▒ 0.05Pb(Mg1/3Nb2/3)O3 -0.05Pb(Zn1/3Nb2/3)O3 -0.90Pb (Zr0.52-Ti0.48)O3의 참조표준 기본정보  
재료규격 조성: 0.05Pb(Mg1/3Nb2/3)O3-0.05Pb(Zn1/3Nb2/3)O3-0.90Pb(Zr0.52-Ti0.48)O3
시편형상 및 제조방법: disk type, 직경 15mm
원료순도: Pb3O4(97%), ZrO2(99%), TiO2(98%), MgCO3(99%), Nb2O5(99.5%), ZnO(99%), Bi2O3(99%), Li2CO3(98%)
혼합 및 분쇄: 볼밀 24h, 미디어 ZrO2
하소/성형/소결:
측정방법 측정/장비: Impedance analyzer(HP4294A), XRD(DMX-2550/pc Rigaku) SEM(Quanta 200), d33(ZJ-3d)
시편형상: Disk, 직경 15mm
▒ 0.05Pb(Mg1/3Nb2/3)O3 -0.05Pb(Zn1/3Nb2/3)O3 -0.90Pb (Zr0.52-Ti0.48)O3의 참조표준 문서자료  
  • [저널정보] MATERIALS SCIENCE & ENGINEERING B / Fabriacation and electrical characteristics of piezoeletric PMN-PZN-PZT ceramic transformer / 138 / / 277-283 ( 2007)

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▒ 0.9Pb0.95Sr0.05 (Zr0.52Ti0.48)O3 - (0.1-x)Pb(Mn1/3Sb2/3)O3 - xPb(Zn1/3Nb2/3)O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.025
참조표준 등급 유효 참조표준
Sample Kp Qm d33
(ρC/N)
εr
(Unpoled)
εr
(poled)
tanδ Tc (℃)
x=0 0.5 2150 190 1000 720 0.0055 225
x=0.02 0.56 1650 220 1100 800 0.005 252
x=0.05 0.64 1350 360 1200 1600 0.0035 272
x=0.07 0.69 200 400 1350 1650 0.0055 300
x=0.1 0.62 100 410 1500 2000 0.013 324
1055
880 227 0.52 976 0.0074 1027
1000 700 231 0.55 1108 0.0069 1040
750 237 0.55 1336 0.0067 1059
780 237 0.55 1562 0.0066 1078
800 241 0.56 1637 0.0063 1102
820 238 0.56 1584 0.0066 1093
850 236 0.55 1535 0.0067 1088
880 228 0.54 1145 0.0068 1055
1020 700 234 0.55 1158 0.0069 1061
750 238 0.56 1736 0.0068 1095
780 244 0.57 1795 0.0064 1095
800 249 0.57 1954 0.0059 1122
820 242 0.57 1822 0.0061 1111
850 236 0.56 1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33), (측정장비 : ZJ-3d) : 0.5(pC/N)
▒ 0.9Pb0.95Sr0.05 (Zr0.52Ti0.48)O3 - (0.1-x)Pb(Mn1/3Sb2/3)O3 - xPb(Zn1/3Nb2/3)O3의 참조표준 기본정보  
재료규격 조성: 0.9Pb0.95Sr0.05 (Zr0.52Ti0.48)O3 - (0.1-x)Pb(Mn1/3Sb2/3)O3 - xPb(Zn1/3Nb2/3)O3 + 0.1 mol% CeO2 (x = 0.00, 0.02, 0.05, 0.07, and 0.10)
시편형상 및 제조방법: disk type, 직경 13mm
원료순도: Pb3O4(97%), ZrO2(99%), TiO2(98%), Nb2O5(99.5%), CeO2(99.5%), SrCO3(9
측정방법 측정/장비: d33 (ZJ-3d, Institute of Acoustics Academic Sinica, China), SEM(Quanta 200, FEI Company), Impedance analyzer( HP 4194A), XRD (DMX-2550/pc, Rigaku, Japan)
시편형상: Disk, 직경 13mm
측정환경: 상온~320℃
▒ 0.9Pb0.95Sr0.05 (Zr0.52Ti0.48)O3 - (0.1-x)Pb(Mn1/3Sb2/3)O3 - xPb(Zn1/3Nb2/3)O3의 참조표준 문서자료  
  • [저널정보] J. Euro. Ceram. Soc. / Structure and electrical properties of PZT-PMS-PZN piezoelectric ceramics / 26 / / 3197-3202 ( 2006)

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▒ 0.05Pb(Mg1/3Nb2/3)O3 -0.05Pb(Zn1/3Nb2/3)O3 - 0.90Pb(Zr0.52Ti0.48)O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.024
참조표준 등급 유효 참조표준
The sintering
temperature(℃)
ZnO and
Li2CO3 (wt%)
Density
(g/㎤)
d33
(ρC/N)
Kp Qm tan δ
(*10-4)
εr r (Ω)
995 0 7.66 224 0.45 1775 79 841 2.93
0.005 7.7 224 0.56 1363 77 861 2.87
0.01 7.75 225 0.57 1467 72 890 2.7
0.015 7.72 222 0.57 1373 74 870 2.98
0.02 7.68 219 0.56 1357 77 868 3.01
1005 0 7.7 245 0.56 1657 78 1032 2.81
0.005 7.75 248 0.57 1666 73 1067 2.86
0.01 7.81 255 0.58 1822 68 1109 2.67
0.015 7.79 249 0.56 1795 72 1072 2.72
0.02 7.81 246 0.55 1773 73 996 2.73
1015 0 7.69 221 0.55 1846 77 883 2.73
0.005 7.73 246 0.56 1408 76 971 2.86
0.01 7.78 249 0.58 1640 71 1046 2.51
0.015 7.74 246 0.57 1528 74 1046 2.62
0.02 7.7 243 0.55 1498 76 991 2.66
1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp),(측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33), (측정장비 : ZJ-3d) : 0.5(pC/N)
▒ 0.05Pb(Mg1/3Nb2/3)O3 -0.05Pb(Zn1/3Nb2/3)O3 - 0.90Pb(Zr0.52Ti0.48)O3의 참조표준 기본정보  
재료규격 조성: 0.05Pb(Mg1/3Nb2/3)O3 - 0.05Pb(Zn1/3Nb2/3)O3 - 0.90Pb(Zr0.52Ti0.48)O3 - 0.10wt % Bi2O3 + xwt %ZnO - Li2CO3 + ywt %Pb3O4, (x or y = 0, 0.005, 0.010, 0.015, 0.020)
시편형상 및 제조방법: disk type, 직경 15mm
원료순도: Pb3O4(97%), ZrO2(99%), TiO2(98%), MgCO3(99%), Nb2O5
측정방법 측정/장비: d33 (ZJ-3d, Institute of Acoustics Academic Sinica, China), SEM(Quanta 200, FEI Company), Impedance analyzer( HP 4294A), XRD (DMX-2550/pc, Rigaku, Japan)
시편형상: Disk, 직경 15mm
측정환경: 상온
▒ 0.05Pb(Mg1/3Nb2/3)O3 -0.05Pb(Zn1/3Nb2/3)O3 - 0.90Pb(Zr0.52Ti0.48)O3의 참조표준 문서자료  
  • [저널정보] SENSORS AND ACTUATORS / Fabrication and characterization of low temperature sintering PMN-PZN-PZT step-down multilayer piezoeletric transformer / / / ( 2008)

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▒ 0.90Pb(Zry-Ti1-y)O3-0.07Pb(Mn1/3Nb2/3)O3-0.03Pb(Ni1/2W1/2)O3 + x wt.%CeO2의 참조표준  
참조표준 번호 KSRD.01.2008.001.023
참조표준 등급 유효 참조표준
Sample Density (g/㎤) Kp Qm d33(ρC/N) εr tanδ
x=0 7.72 0.52 1750 315 1930 0.0057
x=0.1 7.88 0.55 1740 340 1940 0.0058
x=0.2 7.75 0.46 1800 265 1850 0.00575
x=0.3 7.74 0.43 1790 235 1840 0.0058
x=0.4 7.66 0.44 1780 240 1830 0.0061
74 870 2.98
0.02 7.68 219 0.56 1357 77 868 3.01
1005 0 7.7 245 0.56 1657 78 1032 2.81
0.005 7.75 248 0.57 1666 73 1067 2.86
0.01 7.81 255 0.58 1822 68 1109 2.67
0.015 7.79 249 0.56 1795 72 1072 2.72
0.02 7.81 246 0.55 1773 73 996 2.73
1015 0 7.69 221 0.55 1846 77 883 2.73
0.005 7.73 246 0.56 1408 76 971 2.86
0.01 7.78 249 0.58 1640 71 1046 2.51
0.015 7.74 246 0.57 1528 74 1046 2.62
0.02 7.7 243 0.55 1498 76 991 2.66
1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33),(pC/N), (측정장비 : ZJ-3d) : 0.5
▒ 0.90Pb(Zry-Ti1-y)O3-0.07Pb(Mn1/3Nb2/3)O3-0.03Pb(Ni1/2W1/2)O3 + x wt.%CeO2의 참조표준 기본정보  
재료규격 조성: 0.90Pb(Zry-Ti1-y)O3-0.07Pb(Mn1/3Nb2/3)O3-0.03Pb(Ni1/2W1/2)O3 + x wt.%CeO2 (x = 0.0, 0.1, 0.2, 0.3 and 0.4 and y = 52/48, 51/49, 50/50, 49/51, 48/52)
시편형상 및 제조방법: disk type, 직경 15mm
원료순도: Pb3O4(>97%), ZrO2(99%), TiO2(98%), Nb2O5(99.5%), CeO2(99
측정방법 측정/장비: Impedance analyzer/( HP 4294A), SEM/(Model Quanta 200, FEI Company), LCR meter/(Model HP4294A), d33 meter/(Model ZJ-3d, Institute of Acoustics Academic Sinica, China).
시편형상: Disk, 직경 15mm
측정환경: -20~80℃
▒ 0.90Pb(Zry-Ti1-y)O3-0.07Pb(Mn1/3Nb2/3)O3-0.03Pb(Ni1/2W1/2)O3 + x wt.%CeO2의 참조표준 문서자료  
  • [저널정보] CERAMICS INTERNATIONAL / Effects of CeO2 addition on the piezoelectric properties of PNW-PMN-PZT ceramics / / / ( 2008)

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▒ Pb(Mn1/3Nb2/3)0.02(Ni1/3Nb2/3)0.12(Zr0.50Ti0.50)0.86O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.021
참조표준 등급 유효 참조표준
Sintering
Temp(℃)
Dopant 0.2
(wt%)
Density(g/㎤) Dielectric
constant
Kp Qm d33
(ρC/N)
None 7.632 1011 0.59 992 335
850 CuO 7.773 1046 0.59 1000 325
Fe2O3 7.804 1017 0.59 960 319
None 7.697 1105 0.61 1102 355
900 CuO 7.856 1018 0.6 1130 346
Fe2O3 7.85 1275 0.62 975 377
None 7.697 1108 0.62 903 372
950 CuO 7.834 1112 0.61 960 359
Fe2O3 7.832 1405 0.63 949 401
1067 2.86
0.01 7.81 255 0.58 1822 68 1109 2.67
0.015 7.79 249 0.56 1795 72 1072 2.72
0.02 7.81 246 0.55 1773 73 996 2.73
1015 0 7.69 221 0.55 1846 77 883 2.73
0.005 7.73 246 0.56 1408 76 971 2.86
0.01 7.78 249 0.58 1640 71 1046 2.51
0.015 7.74 246 0.57 1528 74 1046 2.62
0.02 7.7 243 0.55 1498 76 991 2.66
1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
▒ Pb(Mn1/3Nb2/3)0.02(Ni1/3Nb2/3)0.12(Zr0.50Ti0.50)0.86O3의 참조표준 기본정보  
재료규격 조성: Pb(Mn1/3Nb2/3)0.02(Ni1/3Nb2/3)0.12(Zr0.50Ti0.50)0.86O3 +0.1wt.%MnO2 + (0.2-X) wt%Fe2O3 + Xwt% CuO + 0.2wt% Na2CO3 + 0.2wt% Li2CO3 (X= 0 and 0.2).
시편형상 및 제조방법: disk type, 직경 21mm
원료 : PbO, ZrO2, TiO2, MnO2, Nb2O5, NiO, CuO and Fe2O3
혼합 및 분쇄: 볼밀 24h
하소/
측정방법 측정/장비: Impedance analyzer(Agilent 4294A)/SEM (Hitachi, S-2400), XRD(Rigaku, D/MAX-2500H)
시편형상: Disk, 직경 21mm
측정환경: 상온~400℃
▒ Pb(Mn1/3Nb2/3)0.02(Ni1/3Nb2/3)0.12(Zr0.50Ti0.50)0.86O3의 참조표준 문서자료  
  • [저널정보] SENSORS AND ACTUATORS / Piezoelectric characteristics of low temperature sintering Pb(Mn1/3Nb2/3)O3 - Pb(Ni1/3Nb2/3)O3 acoording to the addition of CuO and Fe2O3 / A135 / / 215-219 ( 2007)

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▒ Pb1.01[(Mn1/3Nb2/3)0.02(Ni1/3Nb2/3)0.12(Zr0.50Ti0.50)0.86]O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.019
참조표준 등급 유효 참조표준
Sintering Temp(℃) Density (g/㎤) εr Kp(‰) Qm D Grain size (㎛) Tc (℃) Tetragonality c/a
870 7.81 1020 0.583 1059 342 1.211 340 1.021
900 7.88 1095 0.601 1058 363 1.887 340 1.013
930 7.84 1123 0.608 1045 376 1.979 332 1.02
960 7.88 1128 0.61 962 393 2.641 334 1.02
1275 0.62 975 377
None 7.697 1108 0.62 903 372
950 CuO 7.834 1112 0.61 960 359
Fe2O3 7.832 1405 0.63 949 401
1067 2.86
0.01 7.81 255 0.58 1822 68 1109 2.67
0.015 7.79 249 0.56 1795 72 1072 2.72
0.02 7.81 246 0.55 1773 73 996 2.73
1015 0 7.69 221 0.55 1846 77 883 2.73
0.005 7.73 246 0.56 1408 76 971 2.86
0.01 7.78 249 0.58 1640 71 1046 2.51
0.015 7.74 246 0.57 1528 74 1046 2.62
0.02 7.7 243 0.55 1498 76 991 2.66
1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
▒ Pb1.01[(Mn1/3Nb2/3)0.02(Ni1/3Nb2/3)0.12(Zr0.50Ti0.50)0.86]O3의 참조표준 기본정보  
재료규격 조성: Pb1.01[(Mn1/3Nb2/3)0.02(Ni1/3Nb2/3)0.12(Zr0.50Ti0.50)0.86]O3 + 0.1wt% MnO2 + 0.2wt% Li2CO3+0.2wt%Na2CO3
시편형상 및 제조방법: disk type, 직경 21mm, 두께 1mm
원료순도: PbO, MnO2, Nb2O5, NiO, ZrO2, TiO2
혼합 및 분쇄: 볼밀링 24hr, 2차 attrition mill 5hr
하소/성형/소결: 850℃2hr/ (1ton/c
측정방법 측정/장비: XRD,SEM,d33 meter, Impedance Analyzer(Agilent 4294A) LCR-meter(ANDO AG-4304)
시편형상: Disk, 직경 21mm, 두께 1mm
측정환경: 상온~400℃
▒ Pb1.01[(Mn1/3Nb2/3)0.02(Ni1/3Nb2/3)0.12(Zr0.50Ti0.50)0.86]O3의 참조표준 문서자료  
  • [저널정보] Journal of Korean Institute of Electrical and Electronic Material Engineers / Microstructure and Ferroelectric Properties of Low Temperature Sintering PMN-PNN-PZT Ceramics with Sintering Temperature / 19 / 12 / 1118 ( 2006)

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▒ Pb0.98Sr0.02(Mg1/3Nb2/3)x(Mn1/3Nb2/3)y(Zr0.48Ti0.52)zO3의 참조표준  
참조표준 번호 KSRD.01.2008.001.017
참조표준 등급 유효 참조표준
Sintering
temperature (℃)
Sample Density
(g/㎤)
Qm Kp d33(ρC/N)
1220 PMN1 7.57
PMN2 7.67
PMN3 7.54
PMN4 7.47
PMN5 7.42
1240 PMN1 7.67 1940 0.412 255
PMN2 7.75 2160 0.46 270
PMN3 7.85 2380 0.55 308
PMN4 7.8 1790 0.475 282
PMN5 7.72 1650 0.44 248
1260 PMN1 7.51
PMN2 7.55
PMN3 7.62
PMN4 7.7
PMN5 7.77
73 996 2.73
1015 0 7.69 221 0.55 1846 77 883 2.73
0.005 7.73 246 0.56 1408 76 971 2.86
0.01 7.78 249 0.58 1640 71 1046 2.51
0.015 7.74 246 0.57 1528 74 1046 2.62
0.02 7.7 243 0.55 1498 76 991 2.66
1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33), (측정장비 : ZJ-3d) : 0.5(pC/N)
▒ Pb0.98Sr0.02(Mg1/3Nb2/3)x(Mn1/3Nb2/3)y(Zr0.48Ti0.52)zO3의 참조표준 기본정보  
재료규격 조성: Pb0.98Sr0.02(Mg1/3Nb2/3)x(Mn1/3Nb2/3)y(Zr0.48Ti0.52)zO3 + 0.2 wt.%CeO2 (x = 0.06, 0.04 ≤ y ≤ 0.08, 0.86 ≤ z ≤ 0.90, x+y+z = 1 )
시편형상 및 제조방법: disk type, 직경 12mm
원료: Analytical grade oxide powders of PbO, SrCO3, MgO, Nb2O5, ZrO2 and CeO2, and chemical gr
측정방법 측정/장비: XRD/(D/MAX-RB, Rigaku, Japan), 소결특성/밀도,SEM(EPMA-8705QHZ, Japan), 압전특성 /impedance analyzer(Agilent 4294A), d33 meter((Model ZJ-2, China)
시편형상 : 직경 12mm
측정환경: 상온~370℃
▒ Pb0.98Sr0.02(Mg1/3Nb2/3)x(Mn1/3Nb2/3)y(Zr0.48Ti0.52)zO3의 참조표준 문서자료  
  • [저널정보] Materials Chemistry and Physics / Processing and properties of PMMN-PZT quaternary piezoelectric ceramics for ultrasonic motors / 75 / / 202-206 ( 2002)

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▒ 0.35Pb(Zn1/3Nb2/3)O3 ?0.65Pb(ZrxTi1?x)]O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.015
참조표준 등급 유효 참조표준
Sample εr Pr
(μC/㎠)
Kp d31
(10-12C/N)
x=0.43 1460 8 0.38 0.32
x=0.45 1470 12 0.48 0.39
x=0.47 1575 23 0.6 0.53
x=49 1300 15 0.44 0.27
x=0.53 1125 14 0.42 0.22 PMN5 7.42
1240 PMN1 7.67 1940 0.412 255
PMN2 7.75 2160 0.46 270
PMN3 7.85 2380 0.55 308
PMN4 7.8 1790 0.475 282
PMN5 7.72 1650 0.44 248
1260 PMN1 7.51
PMN2 7.55
PMN3 7.62
PMN4 7.7
PMN5 7.77
73 996 2.73
1015 0 7.69 221 0.55 1846 77 883 2.73
0.005 7.73 246 0.56 1408 76 971 2.86
0.01 7.78 249 0.58 1640 71 1046 2.51
0.015 7.74 246 0.57 1528 74 1046 2.62
0.02 7.7 243 0.55 1498 76 991 2.66
1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비 : Solatron SI 1260) : 0.9565
▒ 0.35Pb(Zn1/3Nb2/3)O3 ?0.65Pb(ZrxTi1?x)]O3의 참조표준 기본정보  
재료규격 조성: 0.35Pb(Zn1/3Nb2/3)O3 ?0.65Pb(ZrxTi1?x)]O3 (x = 0.43(M1), 0.45(M2), 0.47(M3), 0.49(M4), 0.53(M5) (Zr/Ti ratio : 43/57, 45/55, 47/53, 49/51, 53/47)
원료: PbO, ZrO2, TiO2, ZnO,Nb2O5.(모두 99%)
혼합 및 분쇄: solid phase reaction
하소/성형/소결: 800℃, 1시간 / 1축 press, 1
측정방법 측정/장비: XRD/(D 5000), 압전특성 /Tc(RLC HIOKI 3532), impedance meter(HP 4193A), (Solatron SI 1260),D-E hysteresis loops(RT66A)
측정환경: 상온~400℃
▒ 0.35Pb(Zn1/3Nb2/3)O3 ?0.65Pb(ZrxTi1?x)]O3의 참조표준 문서자료  
  • [저널정보] Journal of Alloys and Compounds / Some dielectric, ferroelectric, piezoelectric properties of 0.35Pb(Zn1/3Nb2/3)O3 · 0.65Pb(ZrxTi1?x)]O3 ceramics / 449 / / 24-27 ( 2008)

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▒ (Pb0.95Sr0.05) [(Zn1/3Nb2/3)0.20(Zr0.50Ti0.50)0.80)O3 ]+ 0.5wt.%MnO2의 참조표준  
참조표준 번호 KSRD.01.2008.001.014
참조표준 등급 유효 참조표준
εr tanδ Tc (℃) Kp Qm d33
(10-12C/N)
ρ
(g/㎤)
1240 0.002 320 0.62 1360 325 7.78
0.39
x=0.47 1575 23 0.6 0.53
x=49 1300 15 0.44 0.27
x=0.53 1125 14 0.42 0.22 PMN5 7.42
1240 PMN1 7.67 1940 0.412 255
PMN2 7.75 2160 0.46 270
PMN3 7.85 2380 0.55 308
PMN4 7.8 1790 0.475 282
PMN5 7.72 1650 0.44 248
1260 PMN1 7.51
PMN2 7.55
PMN3 7.62
PMN4 7.7
PMN5 7.77
73 996 2.73
1015 0 7.69 221 0.55 1846 77 883 2.73
0.005 7.73 246 0.56 1408 76 971 2.86
0.01 7.78 249 0.58 1640 71 1046 2.51
0.015 7.74 246 0.57 1528 74 1046 2.62
0.02 7.7 243 0.55 1498 76 991 2.66
1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp),(측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33), (측정장비 : ZJ-3d) : 0.5(pC/N)
▒ (Pb0.95Sr0.05) [(Zn1/3Nb2/3)0.20(Zr0.50Ti0.50)0.80)O3 ]+ 0.5wt.%MnO2의 참조표준 기본정보  
재료규격 조성: (Pb0.95Sr0.05)[(Zn1/3Nb2/3)0.20(Zr0.50Ti0.50)0.80)O3 ]+ 0.5wt.%MnO2
시편형상 및 제조방법: disk type, 직경 12mm
원료: Reagent-grade oxide powders, Pb3O4, ZrO2, TiO2, ZnO, Nb2O5, SrCO3 and MnO2
혼합 및 분쇄: columbite precursor method, 습식혼합, 볼밀, 24hr, ethanol
하소/성형/소결: 1
측정방법 측정/장비: XRD/(DMX-IIIC, Japan), 소결특성/밀도,SEM(Hitachi S-570, Japan) 압전특성/d33 meter ((ZJ-3D, Institute of Acoustics Academic Sinica, China),impedance analyzer(Agilent 4294A)
시편형상 : 직경 12mm
측정환경: 상온~370℃
▒ (Pb0.95Sr0.05) [(Zn1/3Nb2/3)0.20(Zr0.50Ti0.50)0.80)O3 ]+ 0.5wt.%MnO2의 참조표준 문서자료  
  • [저널정보] Materials Letters / Piezoelectric properties of new MnO2-added 0.2 PZN-0.8 PZT ceramic / 58 / / 1508- 1512 ( 2004)

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▒ 0.2Pb(Zn1/3Nb2/3)O3-0.8Pb (Zr0.5Ti0.5)O3 + xWO3의 참조표준  
참조표준 번호 KSRD.01.2008.001.012
참조표준 등급 유효 참조표준
Samples Ec(V/㎜) Pr(μC/㎠) Ps(μC/㎠)
P1# 918 30.09 37.98
P2# 909 26.21 35.02
P3# 812 18.78 28.73
P4# 802 18.19 27.91 x=49 1300 15 0.44 0.27
x=0.53 1125 14 0.42 0.22 PMN5 7.42
1240 PMN1 7.67 1940 0.412 255
PMN2 7.75 2160 0.46 270
PMN3 7.85 2380 0.55 308
PMN4 7.8 1790 0.475 282
PMN5 7.72 1650 0.44 248
1260 PMN1 7.51
PMN2 7.55
PMN3 7.62
PMN4 7.7
PMN5 7.77
73 996 2.73
1015 0 7.69 221 0.55 1846 77 883 2.73
0.005 7.73 246 0.56 1408 76 971 2.86
0.01 7.78 249 0.58 1640 71 1046 2.51
0.015 7.74 246 0.57 1528 74 1046 2.62
0.02 7.7 243 0.55 1498 76 991 2.66
1693 0.0065 1084
880 235 0.55 1659 0.0068 1026
1040 700 233 0.55 1386 0.0066 1040
750 234 0.55 1578 0.0065 1041
780 241 0.55 1667 0.0064 1080
800 243 0.56 1755 0.0061 1117
820 241 0.55 1636 0.0066 1103
850 235 0.55 1558 0.0068 1059
880 235 0.55 1417 0.0075 1031
1060 700 232 0.54 1348 0.0064 1011
750 233 0.55 1370 0.0064 1025
780 240 0.55 1435 0.0064 1053
800 241 0.56 1753 0.0063 1061
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp),(측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33),(측정장비 : ZJ-3d) : 0.5(pC/N)
▒ 0.2Pb(Zn1/3Nb2/3)O3-0.8Pb (Zr0.5Ti0.5)O3 + xWO3의 참조표준 기본정보  
재료규격 조성 : 0.2Pb(Zn1/3Nb2/3)O3-0.8Pb (Zr0.5Ti0.5)O3 + xWO3 wt% (x = 0, 0.5, 1, 1.5)
시편형상 및 제조방법: disk type, 직경 12mm
원료순도: Reagent-grade oxide powders, Pb3O4, ZnO, Nb2O5, ZrO2, TiO2, WO3
혼합 및 분쇄: two-step method, 습식혼합, 볼밀, ZrO2 ball
하소/성형/소결: 1100℃, 4시간, 850℃,
측정방법 측정/장비: XRD(DMX-IIC, Japan), SEM(Hitachi S-570, Japan), impedance analyzer (HP 4294A), LCR meter (HP4284, Hewlett-Packard), d33 meter ((ZJ-3D, Institute of Acoustics Academic Sinica, China)
시편형상 : 직경 12mm
측정환경: 상온
▒ 0.2Pb(Zn1/3Nb2/3)O3-0.8Pb (Zr0.5Ti0.5)O3 + xWO3의 참조표준 문서자료  
  • [저널정보] Ceramics International / Effect of tungsten on the structure and piezoelectric properties of PZN-PZT ceramics / 33 / / 1019-1023 ( 2007)

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▒ Pb(Zr,Ti)O3-Pb(Fe2/3W1/3)O3-Pb(Mn1/3Nb2/3)O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.010
참조표준 등급 유효 참조표준
Sintering
temperature (℃)
Sample Kp Qm d33
(ρC/N)
tanδ Tc (℃) Density
(g/㎤)
980 x=0 0.355 850 200 0.0074 7.46
x=0.1 0.37 900 210 0.007 7.48
x=0.15 0.4 980 220 0.0068 7.67
x=0.2 0.47 1050 240 0.0066 7.7
x=0.3 0.51 1150 275 0.0062 7.75
x=0.5 0.42 920 240 0.007 7.65
x=0.7 0.4 500 220 0.0078 7.5
1020 x=0 0.41 1190 215 0.0068 272 7.47
x=0.1 0.43 1200 230 0.006 292 7.55
x=0.15 0.47 1250 240 0.0059 294 7.72
x=0.2 0.55 1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp),(측정장비 : HP 4294A) : 0.02259
측정불확도: 압전 상수(d33), (측정장비 : ZJ-3d) : 0.5(pC/N)
▒ Pb(Zr,Ti)O3-Pb(Fe2/3W1/3)O3-Pb(Mn1/3Nb2/3)O3의 참조표준 기본정보  
재료규격 조성 : Pb(Zr,Ti)O3-Pb(Fe2/3W1/3)O3-Pb(Mn1/3Nb2/3)O3 + 0.2 wt.% CeO2 + 2.0 wt.% Pb3O4 +x wt.% YMnO3 (x = 0.0, 0.10, 0.15, 0.20, 0.30, 0.50, 0.70)
시편형상 및 제조방법: disk type, 직경 15mm
원료순도: Pb3O4 (97%), ZrO2(99%),TiO2 (98%), SrCO3 (99%), Nb2O5 (99.5%), MnCO3 (96.2
측정방법 측정/장비: XRD/Rigaku Minifiex Japan, 유전율 유전손실/HP 4623B LCR meter 압전특성 /Siemens Impedance Bridge-Type R207, d33-meter model CPDT 3300 (Channel Products Inc., USA)
시편형상 : 직경 10mm, 두께 1~2mm
측정환경: 상온~600K
▒ Pb(Zr,Ti)O3-Pb(Fe2/3W1/3)O3-Pb(Mn1/3Nb2/3)O3의 참조표준 문서자료  
  • [저널정보] Materials Research Bulletin / Low temperature sintering and properties of piezoelectric PZT-PFW-PMN ceramics with YMnO3 addition / 32 / / 38-44 ( 2008)

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▒ Pb0.98Sr0.02(Mn1/3Sb2/3)yZrzTi1-y-zO3의 참조표준  
참조표준 번호 KSRD.01.2008.001.008
참조표준 등급 유효 참조표준
Sintering
temperature(℃)
εr d33(ρC/N) kp Qm tanδ (%)
1100 1140 310 0.53 1755 0.75
1150 1370 348 0.57 1620 0.62
1200 1470 365 0.59 1325 0.45
1240 1530 374 0.6 1250 0.41
7.67
x=0.2 0.47 1050 240 0.0066 7.7
x=0.3 0.51 1150 275 0.0062 7.75
x=0.5 0.42 920 240 0.007 7.65
x=0.7 0.4 500 220 0.0078 7.5
1020 x=0 0.41 1190 215 0.0068 272 7.47
x=0.1 0.43 1200 230 0.006 292 7.55
x=0.15 0.47 1250 240 0.0059 294 7.72
x=0.2 0.55 1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도 : 전기기계 결합계수(kp), (측정장비 : HP 4294A) : 0.02259
▒ Pb0.98Sr0.02(Mn1/3Sb2/3)yZrzTi1-y-zO3의 참조표준 기본정보  
재료규격 조성 : Pb0.98Sr0.02(Mn1/3Sb2/3)yZrzTi1-y-zO3 (0 < y < 0.10, 0.4 < z < 0.5)
시편형상 및 제조방법: disk type, 직경 12mm, 두께 1.5mm
원료순도: Pb3O4,SrCO3, MnCO3, Sb2O3, ZrO2, and TiO2(>99.0%)
혼합 및 분쇄: 습식혼합, 볼밀, 6hr,
하소/성형/소결: 800℃, 2시간/ 1축 press, 200 kg/cm2/1100~1300℃, 2시간전
측정방법 측정/장비: XRD/Rigaku Minifiex Japan, 유전율 유전손실/HP 4623B LCR meter 압전특성 /Siemens Impedance Bridge-Type R207, d33-meter model CPDT 3300 (Channel Products Inc., USA)
시편형상 : 직경 10mm, 두께 1~2mm
측정환경: 상온~600K
▒ Pb0.98Sr0.02(Mn1/3Sb2/3)yZrzTi1-y-zO3의 참조표준 문서자료  
  • [저널정보] Materials Science and Engineering B / Microstructure and piezoelectric properties of PMS?PZT ceramics / 117 / / 216-220 ( 2005)

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▒ 0.2[Pb(Mg1/3Nb2/3)]-0.8[PbTiO3-PbZrO3]의 참조표준  
참조표준 번호 KSRD.01.2008.001.006
참조표준 등급 유효 참조표준
Density
(g/㎤)
phase
(T/R)
εr at RT tanδ at RT Tc (℃) Pr(μC/㎠) Ec(kV/㎝) kp(%) d33(ρC/N) K33(%) Qm σ * 10-12
(Ω㎝)-1
PMN-PZT 1100℃ 7.7535 1.68 1420 0.0216 327 13.6 4.5 56.6 406 ­ 82.7 ­
PMN-PZT 950℃ 7.521 2.19 716 0.038 336 0.8 5.07 19.9 152 25.7 66.2 2.42
0.05wt% Li2O 7.837 1.24 1431 0.021 322 26.26 7.61 41.3 405 70.2 67.7 2.63
0.1wt% Li2O 7.8423 1.16 1448 0.022 322 27.16 8.27 63.7 527 77.9 77 4.26
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp),(측정장비 : Solatron SI 1260) : 0.9565
▒ 0.2[Pb(Mg1/3Nb2/3)]-0.8[PbTiO3-PbZrO3]의 참조표준 기본정보  
재료규격 조성: 0.2[Pb(Mg1/3Nb2/3)]?0.8[PbTiO3?PbZrO3] + x Li2Owt% (x=0, 0.05, 0.1, 0.2, 0.3)
시편형상 및 제조방법: disk type, 직경 18mm
원료: PbO, MgO,Nb2O5, ZrO2 and TiO2, Li2O
혼합 및 분쇄: two-step solid-state reaction method, 습식혼합, 볼밀, 24hr,
하소/성형/소결: 1000℃, 4시간 , 850℃, 2시간/
측정방법 측정/장비: XRD/(XRD RAD III, Rigaku, Japan), 소결특성/밀도,(SEM-EDS, S-4200, Hitachi, Japan), 압전특성 /impedance analyzer(Agilent 4192A), (Solatron SI 1260)
시편형상 : 직경 18mm
측정환경: 상온~400℃
▒ 0.2[Pb(Mg1/3Nb2/3)]-0.8[PbTiO3-PbZrO3]의 참조표준 문서자료  
  • [저널정보] Materials Chemistry and Physics / Conduction analysis of Li2O doped 0.2[Pb(Mg1/3Nb2/3)]?0.8[PbTiO3?PbZrO3] ceramics fabricated by columbite precursor method / 90 / / 381-385 ( 2005)

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▒ 0.94(K0.5Na0.5)NbO3-0.06LiNbO3의 참조표준  
참조표준 번호 KSRD.01.2008.001.003
참조표준 등급 유효 참조표준
Kp Kt d33(ρC/N) Pr(μC/㎠) Ec(kV/㎝) Tc(℃)
0.38 0.48 215 20 13.4 450
σ * 10-12
(Ω㎝)-1
PMN-PZT 1100℃ 7.7535 1.68 1420 0.0216 327 13.6 4.5 56.6 406 ­ 82.7 ­
PMN-PZT 950℃ 7.521 2.19 716 0.038 336 0.8 5.07 19.9 152 25.7 66.2 2.42
0.05wt% Li2O 7.837 1.24 1431 0.021 322 26.26 7.61 41.3 405 70.2 67.7 2.63
0.1wt% Li2O 7.8423 1.16 1448 0.022 322 27.16 8.27 63.7 527 77.9 77 4.26
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 전기기계 결합계수(kp), (측정장비:HP 4294A) : 0.02259
▒ 0.94(K0.5Na0.5)NbO3-0.06LiNbO3의 참조표준 기본정보  
재료규격 조성: 0.94(K0.5Na0.5)NbO3-0.06LiNbO3
시편형상 및 제조방법: disk type, 직경 12mm, 두께 1mm
원료: K2CO3, Na2CO3, Li2CO3 and Nb2O5(Reagent-grade oxid, carbonate powder
혼합 및 분쇄: 습식혼합, planetary milling, 24시간, alcohol
하소/성형/소결: 850℃, 5시간/ 1축 press,300MPa/1060~1100℃, 2시간
전극: Si
측정방법 측정/장비: XRD/Philips X-Pert Diffractormeter, SEM/JSM-6360, Japan, 강유전특성 /Radiant Precision Workstation, 압전특성 /impedance analyzer (Agilent 4294)
시편형상 : 직경 12mm, 두께 1mm
측정환경: 상온
▒ 0.94(K0.5Na0.5)NbO3-0.06LiNbO3의 참조표준 문서자료  
  • [저널정보] Materials Science and Engineering B / Effect of poling condition on piezoelectric properties of (K0.5Na0.5)NbO3-LiNbO3 lead-free piezoelectric ceramics / 137 / / 175-179 ( 2007)

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▒ (Pb0.85-xCdxSm0.1)(Ti0.98Mn0.02)O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.001
참조표준 등급 유효 참조표준
Cd content
[mol%]
εr tan δ Kt kp Nt
(Hz m)
Np
(Hz m)
x = 0.01 212 9×10-3 0.54 0.042 2091 2757
x = 0.02 221 8×10-3 0.557 0.036 2056 2762
x = 0.03 220 7×10-3 0.562 0.041 2003 2736
x = 0.04 222 8×10-3 0.55 0.044 2037 2750
x = 0.05 218 7.5×10-3 0.544 0.047 2068 2788
x = 0.08 226 8×10-3 0.532 0.048 2069 2816
70.2 67.7 2.63
0.1wt% Li2O 7.8423 1.16 1448 0.022 322 27.16 8.27 63.7 527 77.9 77 4.26
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도 : 전기기계 결합계수(kp),(측정장비: HP 8714ES) : 0.00564
▒ (Pb0.85-xCdxSm0.1)(Ti0.98Mn0.02)O3의 참조표준 기본정보  
재료규격 조성: (Pb0.85-xCdxSm0.1)(Ti0.98Mn0.02)O3 (x=0.01-0.08)
시편형상 및 제조방법: plate, 20×20×1 mm3,, 12 mm diameter and 1 mm thickness,
원료순도: PbO, TiO2, Sm2O3, CdO, MnO2 powders (>99.0%purity)
혼합 및 분쇄: 습식혼합, 볼밀 6시간
하소/성형/소결: 900℃, 2시간/ 1축 press, 25MPa/1150℃, 2시간, Pb
측정방법 측정/장비: XRD/Rigaku D/MAX2 500, SEM/Hitachi S4100, 압전특성/impedance analyzer(HP4192). )network analyzer (HP 8714ES)
시편형상: 12 mm diameter and 1 mm thickness,
측정환경: 상온(25℃) 및 환경시험(25~80℃)
▒ (Pb0.85-xCdxSm0.1)(Ti0.98Mn0.02)O3의 참조표준 문서자료  
  • [저널정보] J. Euro. Ceram. Sco. / The influence of Cd doping on the surface acoustic wave properties of Sm-modified PbTiO3 ceramics / 24 / / 1993-1998 ( 2004)

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▒ (1-x)PNZ-xBT ceramics derived from mechanochemically synthesized powders의 참조표준  
참조표준 번호 KSRD.01.2008.001.022
참조표준 등급 유효 참조표준
Composition
(1-x)PZN-(x)BT
Perovskite
Percent (%)
Grain size
(um)
Relative
Density [%]
Dielectric
Constant [εr]
x = 0.0 95 4.5 93 3105
x = 0.05 100 3.1 95 4623
x = 0.15 100 2.6 95 9254
x = 0.20 100 2.1 96 5983
x = 0.25 100 1.6 96 4135
x = 0.30 100 1.2 97 3306
x = 0.05 218 7.5×10-3 0.544 0.047 2068 2788
x = 0.08 226 8×10-3 0.532 0.048 2069 2816
70.2 67.7 2.63
0.1wt% Li2O 7.8423 1.16 1448 0.022 322 27.16 8.27 63.7 527 77.9 77 4.26
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비:? HP4194A): 28.44
▒ (1-x)PNZ-xBT ceramics derived from mechanochemically synthesized powders의 참조표준 기본정보  
재료규격 - 조성: (1-x)Pb(Zn1/3Nb2/3)O3-xBaTiO3, (x = 0 ~ 0.3)
- 시편형상 및 제조방법: Disk 직경 10mm, 두께 1mm
- 원료순도: PbO (>99.9%), Nb2O5 (>99%), ZnO (>99%), BaCO3 (>99%), and TiO2 (>99.9%)
- 혼합 및 분쇄: Planetary mill (12h/매25분후 5분간 정지/200rpm),
측정방법 - 측정/장비: 유전특성 Impedance Analyzer(HP4194)
- 시편형상: 재료규격 참조
- 소결특성: Mirage MD-200S type electronic densimeter
- 측정환경: 주파수 kHz
▒ (1-x)PNZ-xBT ceramics derived from mechanochemically synthesized powders의 참조표준 문서자료  
  • [저널정보] Materials Research Bulletin / (1?x)PNZ?xBT ceramics derived from mechanochemically synthesized powders / 37 / / 1085 ( 2002)

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▒ Dielectric properties of (1-x)Pb(Zr0.52Ti0.48)O3 ? (x)BaTiO3 ceramics under uniaxial compressive pre-stress의 참조표준  
참조표준 번호 KSRD.01.2008.001.020
참조표준 등급 유효 참조표준
Composition
(1-x)PZT-(x)BT
Density
[g/cm3]
Average Grain
size (um)
Dielectric Constant
Stress-free [εr]
Loss Tangent
Stress-free [tanδ]
x = 0.0 7.75 1.89 ± 0.52 813 0.011
x = 0.05 7.67 1.66 ± 0.32 809 0.007
x = 0.15 7.42 2.40 ± 0.58 839 0.006
x = 0.25 7.3 1.91 ± 0.47 857 0.004
x = 0.35 6.99 2.36 ± 0.71 875 0.005
x = 0.45 6.78 2.93 ± 0.53 890 0.006
x = 0.55 6.63 3.17 ± 0.72 952 0.005
x = 0.65 6.38 4.42 ± 0.79 1060 0.007
x = 0.75 6.28 3.28 ± 0.53 1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비: HP7276A): 3.32
▒ Dielectric properties of (1-x)Pb(Zr0.52Ti0.48)O3 ? (x)BaTiO3 ceramics under uniaxial compressive pre-stress의 참조표준 기본정보  
재료규격 - 조성: (1-x)Pb(Zr0.52Ti0.48)O3- (x)BaTiO3 ceramics
- 시편형상 및 제조방법: Disk, 직경 10mm, 두께 2mm
- 원료순도: PbO(99%), ZrO2(99%), TiO2(99%), BaCO3(99%) and TiO2(99%)
- 혼합 및 분쇄: [PZT] ball mill (3h), 미디어 ZrO2, 용매 에탄올 [BT] ball mill (24h), 미디어 ZrO
측정방법 - 측정/장비: 유전특성 LCZ meter(HP 7276A)
- 시편형상: 재료규격 참조
- 소결밀도: Archimedes법
- 측정환경: 유전특성 25oC, 1kHz
▒ Dielectric properties of (1-x)Pb(Zr0.52Ti0.48)O3 ? (x)BaTiO3 ceramics under uniaxial compressive pre-stress의 참조표준 문서자료  
  • [저널정보] Materials chemistry and physics / Dielectric properties of (1-x)Pb(Zr0.52Ti0.48)O3 ? (x)BaTiO3 ceramics under uniaxial compressive pre-stress / 102 / / 165 ( 2007)

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▒ Low temperature sintering and dielectric properties of (Ba,Ca) (Ti,Li)(O,F)3 ceramics with high permittivity의 참조표준  
참조표준 번호 KSRD.01.2008.001.018
참조표준 등급 유효 참조표준
Sintering
Temperature (oC)
Sintering
Time (h)
Sintering
Shrinkage (%)
Relative Dielectric
Constant [εr]
Loss Tangent
[tanδ]
Curie Temp.
[Tc]
800 2 7 980 0.006 368
930 2 11.7 3100 0.01 288
1000 2 12.5 3500 0.008 293
1100 2 12.5 2820 0.007 273
930 4 11.7 4250 0.007 288
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비: HP 4191A): 14.98
▒ Low temperature sintering and dielectric properties of (Ba,Ca) (Ti,Li)(O,F)3 ceramics with high permittivity의 참조표준 기본정보  
재료규격 - 조성: BaTiO3 (95mol%), CaF2 (2.5 mol%), LiF(2.5 mol%)
- 시편형상 및 제조방법: Disk, 직경 13mm, 두께 1mm
- 원료순도: BaCO3 (99%) and TiO2 (99%), and super pure CaF2 and LiF2
- 혼합 및 분쇄: Hand milling, 1h
- 하소/성형/소결: /1축 press, 100MPa/800~1100oC, 2~8h, 승온속도 200oC/h
- 전극:
측정방법 - 측정/장비: 고주파 유전특성 Impedance Analyzer(HP4191A)
- 시편형상: 재료규격 참조
- 소결특성: 소결수축율 대체
- 측정환경: 실온, 100Hz ~ 40MHz
▒ Low temperature sintering and dielectric properties of (Ba,Ca) (Ti,Li)(O,F)3 ceramics with high permittivity의 참조표준 문서자료  
  • [저널정보] Solid State Sciences / Low temperature sintering and dielectric properties of (Ba,Ca) (Ti,Li)(O,F)3 ceramics with high permittivity / 8 / / 922 ( 2006)

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▒ Structural and dielectric properties of Sb2O3-doped (Ba0.992?xSrxY0.008) TiO3.004 ceramics의 참조표준  
참조표준 번호 KSRD.01.2008.001.016
참조표준 등급 유효 참조표준
Composition
(Ba0.732Sr0.26Y0.008)TiO3.004
+ x Sb2O3 (wt%)
Theoretical
Density (g/cm3)
Density
(%)
Curie Temp.
[Tc]
x = 0 5.79 94 37
x = 0.8 5.82 95 9
x = 1.2 5.83 95 -3
x = 1.6 5.84 96 below-30
x = 2.0 5.85 96 below-30
1100 2 12.5 2820 0.007 273
930 4 11.7 4250 0.007 288
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: Curie온도, 1.0oC
▒ Structural and dielectric properties of Sb2O3-doped (Ba0.992?xSrxY0.008) TiO3.004 ceramics의 참조표준 기본정보  
재료규격 - 조성: (Ba0.732Sr0.26Y0.008)TiO3.004 + x wt% Sb2O3, (x = 0, 0.8, 1.2, 1.6, 2.0)
- 시편형상 및 제조방법: Disk, 직경 10mm, 두께 2mm
- 원료순도:BaCO3 (>99.0%), SrCO3 (>99.0%), TiO2 (>98.0%) and Y2O3 (>99.5%)
- 혼합 및 분쇄: ball mill
- 하소/성형/소결: 1080oC, 2h/1축 press, 250MPa, P
측정방법 - 측정/장비: 유전특성 LCR meter(4425)
- 시편형상: 재료규격 참조
- 소결특성: 미세구조 관찰 대체
- 측정환경: 1kHz
▒ Structural and dielectric properties of Sb2O3-doped (Ba0.992?xSrxY0.008) TiO3.004 ceramics의 참조표준 문서자료  
  • [저널정보] Material Science and Engineering: B / Structural and dielectric properties of Sb2O3-doped (Ba0.992?xSrxY0.008) TiO3.004 ceramics / 136 / / 118 ( 2007)

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▒ Effects of alumina nano-particulates addition on mechanical and electrical properties of barium titanate ceramics의 참조표준  
참조표준 번호 KSRD.01.2008.001.013
참조표준 등급 유효 참조표준
Composition
BaTiO3 + xAl2O3 (Vol.%)
Relative
Density (%)
Grain Size
(um)
Relative Dielectric
Constant [εr]
Loss Tangent
[tanδ]
Curie Temperature
Tc (oC)
x = 0 93.5 52.5 1606 0.0078 120
x = 0.5 93.5 49.8 1602 0.0078 121
x = 1 93 47 1581 0.0124 118
x = 3 89.7 39.9 1213 0.0339 121
x = 5 88.1 37.2 942 0.0451 125
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비:HP 4284A): 2.89
?측정불확도: tanδ, (측정장비: HP 4284A): 0.00032
▒ Effects of alumina nano-particulates addition on mechanical and electrical properties of barium titanate ceramics의 참조표준 기본정보  
재료규격 - 조성: BaTiO3 + xAl2O3 (x = 0, 0.5, 1, 3 and 5 vol%)
- 시편형상 및 제조방법: Disk
- 원료순도: BaTiO3 (house prepared), Al2O3 (Aldrich, ~40nm)
- 혼합 및 분쇄: 초음파 분산 20min, ball mill (24h)
- 하소/성형/소결: /1축 press, PVA 3%/1450oC, 2h, 승온 및 하강속도 5oC/min
- 전극: Silver p
측정방법 - 측정/장비: 유전특성 LCR meter(HP4284A)
- 시편형상: 재료규격 참조
- 소결특성: Archimedes법
- 측정환경: 상온, 1kHz
- 미세구조: 결정립크기 linear intercept method
▒ Effects of alumina nano-particulates addition on mechanical and electrical properties of barium titanate ceramics의 참조표준 문서자료  
  • [저널정보] Current Applied Physics / Effects of alumina nano-particulates addition on mechanical and electrical properties of barium titanate ceramics / 8 / / 48 ( 2008)

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▒ Dielectric and ferroelectric characteristics of barium zirconate titanate ceramics prepared from mixed oxide method의 참조표준  
참조표준 번호 KSRD.01.2008.001.011
참조표준 등급 유효 참조표준
Composition
Ba(Ti1-xZrx)O3
BZT Powder
Surface Area (nm)
Remenant
Polarization Pr (uC/cm2)
Coerive Field
Ec (kV/cm)
Max. Dielectric
Permittivity at 100kHz
x = 0.05 0.83 5.4 186 14400
x = 0.10 0.27 5.3 134 11660
x = 0.15 0.16 3.6 157 5300 47 1581 0.0124 118
x = 3 89.7 39.9 1213 0.0339 121
x = 5 88.1 37.2 942 0.0451 125
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비: HP 4192): 15.32
▒ Dielectric and ferroelectric characteristics of barium zirconate titanate ceramics prepared from mixed oxide method의 참조표준 기본정보  
재료규격 - 조성: Ba(Ti1-xZrx)O3 (x = 0.05, 0.1, 0.15)
- 시편형상 및 제조방법: Disk, 직경 12mm, 두께 1mm
- 원료순도: BaCO3(Vetec), ZrO2(Inlab), TiO2 (Vetec) Analytic grade
- 혼합 및 분쇄: ball mill, 용매 Isopropyl Alcohol
- 하소/성형/소결: /1축 press, 210MPa/1550oC, 4h
- 전극: Gold elec
측정방법 - 측정/장비: 유전특성 Impedance Analyzer(HP 4192)
- 시편형상: 재료규격 참조
- 소결수축율: Dilatometer
- 측정환경: 유전특성 100kHz
▒ Dielectric and ferroelectric characteristics of barium zirconate titanate ceramics prepared from mixed oxide method의 참조표준 문서자료  
  • [저널정보] J. Alloys and Compounds / Dielectric and ferroelectric characteristics of barium zirconate titanate ceramics prepared from mixed oxide method / 462 / / 129 ( 2008)

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▒ Structure and dielectric behavior of Nd-doped BaTiO3 perovskites의 참조표준  
참조표준 번호 KSRD.01.2008.001.009
참조표준 등급 유효 참조표준
Material Composition
Ba1?xNdxTiO3
Relative
Density (%)
Average Grain
Size (um)
Curie Temperature
Tc (oC)
S1 x = 0 97.1 1.8 128
S2 x = 0.005 97 1.2 109
S3 x = 0.01 97.3 0.8 98
x = 0.02 96.9 0.7 76
x = 0.05 96.7 0.7 15
x = 0.10 96.3 0.6 -25
125
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: Curie온도 1.0oC
▒ Structure and dielectric behavior of Nd-doped BaTiO3 perovskites의 참조표준 기본정보  
재료규격 - 조성: Ba1-xNdxTiO3 (0 ≤ x ≤ 0.10)
- 시편형상 및 제조방법: Disk, 직경 12mm, 두께 2mm
- 원료순도: BaCO3(>99.0%), TiO2(>99.0%), Nd2O3 (99.9%)
- 혼합 및 분쇄: ball mill (48h), 미디어 ZrO2, 용매 Isopropyl Alcohol
- 하소/성형/소결:1100oC, 4h/1축 press 200MPa/1250~1400oC, 3h
- 전극: Silve
측정방법 - 측정/장비: 유전특성 LCR meter(HP 4284A), XRD(Philips, PW3050/60)
- 시편형상: 재료규격 참조
- 소결밀도: Archimedes법
- 측정환경: 유전특성-30 ~ 160oC, 1 ~ 500kHz
▒ Structure and dielectric behavior of Nd-doped BaTiO3 perovskites의 참조표준 문서자료  
  • [저널정보] Materials Chemistry and Physics / Structure and dielectric behavior of Nd-doped BaTiO3 perovskites / 109 / / 475 ( 2008)

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▒ Grain growth control in Nb-doped BaTiO3의 참조표준  
참조표준 번호 KSRD.01.2008.001.007
참조표준 등급 유효 참조표준
Material Density
[%]
Grain size
(um)
Predominant
structure
Rsistivity
[Ωcm]
Relative Dielectric
Constant [εr]
Loss Tangent
[tanδ]
S1 81 5 psudocubic >108 2200 1.6
S2 94 2 psudocubic >108 2500 3.2
S3 95 >50 tetragonal 44 300000 25
0.7 15
x = 0.10 96.3 0.6 -25
125
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비: HP 4284A): 1.60
측정불확도: tanδ, (측정장비 : HP 4284A): 0.00036
▒ Grain growth control in Nb-doped BaTiO3의 참조표준 기본정보  
재료규격 - 조성: BaTiO3 + (0.15 mole%)Nb2O5(유전특성)
- 시편형상 및 제조방법: Disk, 직경 10mm, 두께 2mm
- 원료순도: BaCO3(Lennox Lab. Inc.), TiO2(Degussa, Baker chem. co.), Nb2O5(Fluka A.G.)--> 원료의 메이커 및 입경 표기됨
- 혼합 및 분쇄: Planetary mill (4h, 10h), 미디어 ZrO2, 용매 Isopropy
측정방법 - 측정/장비: 유전특성 LCR meter(HP 4284A); 비저항 Electrometer(Keithley614)
- 시편형상: 재료규격 참조
- 소결밀도: Archimedes법
- 측정환경: 유전특성 25~125oC, 1 and 100kHz; 비저항 DC 10V
▒ Grain growth control in Nb-doped BaTiO3의 참조표준 문서자료  
  • [저널정보] J. Materials Processing? Technology / Grain growth control in Nb-doped BaTiO3 / 168 / / 464 ( 2005)

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▒ Structural and dielectric properties of the system Ba1?xSrxFe0.01Ti0.99O3의 참조표준  
참조표준 번호 KSRD.01.2008.001.005
참조표준 등급 유효 참조표준
Composition Lattice
Parameter (A)
Density
(g/cm3)
Grain Size
(um)
Relative Dielectric
Constant(εr)
Loss tangent
[tanδ]
Curie Temperature
Tc (oC)
x = 0.30 3.9732 5.39 11 4065 0.017 13
x = 0.40 3.9612 5.34 9 1865 0.009 -14
x = 0.55 3.9441 5.26 5 880 0.005 -60
0.7 15
x = 0.10 96.3 0.6 -25
125
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비: HP 4284A): 4.7
측정불확도: tanδ, (측정장비: HP 4284A): 0.00026
▒ Structural and dielectric properties of the system Ba1?xSrxFe0.01Ti0.99O3의 참조표준 기본정보  
재료규격 - 조성: Ba1-xSrxFe0.01Ti0.99O3 (x = 0.3, 04, 0.55)
- 시편형상 및 제조방법: Disk, 직경 10mm, 두께 0.5mm
- 원료순도: BaCO3 (99.9%), SrCO3, TiO2 (99.9%) and Fe2O3 (99.9%)
- 혼합 및 분쇄: Ball mill, 24h,, 미디어 ZrO2, 용매 증류수
- 하소/성형/소결: 1000oC, 4h/CIP, 100MPa/1450oC, 4h, 승온속도 2oC
측정방법 - 측정/장비: 유전특성 LCR meter (HP 4284A)
- 시편형상: 재료규격 참조
- 소결특성: 소결밀도
- 측정환경: 1kHz
▒ Structural and dielectric properties of the system Ba1?xSrxFe0.01Ti0.99O3의 참조표준 문서자료  
  • [저널정보] Materials Letters / Structural and dielectric properties of the system Ba1?xSrxFe0.01Ti0.99O3 / 57 / / 3003 ( 2003)

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▒ BST ceramics: Effect of attrition milling on dielectric properties의 참조표준  
참조표준 번호 KSRD.01.2008.001.004
참조표준 등급 유효 참조표준
Sintering
Method
Sintering Condition
Temperature/Time (oC/h)
Grain
Size (nm)
Theoretical
Density (%)
Relative Dielectric
Constant(εr)
Loss tangent
[tanδ]
HUP 1100/1 130 77 1120 0.017
HUP 1150/1 410 97 1880 0.018
HUP 1200/1 465 98 3170 0.006
Conventional 1400/5 1265 90 3150 0.0009
Conventional 1465/5 >?10000 92 4410 0.0011
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비: HP 4194A): 29.88
▒ BST ceramics: Effect of attrition milling on dielectric properties의 참조표준 기본정보  
재료규격 - 조성: Ba0.6Sr0.4TiO3
- 시편형상 및 제조방법: Disk, 직경 10mm, 두께 1mm
- 원료순도: BaCO3 (Merck 1711), SrCO3 (Prolabo 28311.297) and TiO2 (Toho 113)
- 혼합 및 분쇄: Turbula milling, 4h, 미디어 yttria zirconia(직경12mm), 용매 증류수 [하소분말] Turbula milling, 4h, 미디어 yttria zir
측정방법 - 측정/장비: 고주파 유전특성 Impedance Analyzer(HP4194A)
- 시편형상: 재료규격 참조
- 소결특성: 미세구조 대체
- 측정환경:-60 ~ 150oC, 10kHz ~ 10MHz
▒ BST ceramics: Effect of attrition milling on dielectric properties의 참조표준 문서자료  
  • [저널정보] J. Euro. Ceram. Soc. / BST ceramics: Effect of attrition milling on dielectric properties / 24 / / 3003 ( 2004)

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▒ Influence of Bi2O3 and CuO addition on low-temperature sintering and dielectric properties of Ba0.6Sr0.4TiO3 ceramics의 참조표준  
참조표준 번호 KSRD.01.2008.001.002
참조표준 등급 유효 참조표준
Sample
Name
Relative Dielectric
Constant εr(10kHz)
Loss tangent?
tanδ(10kHz)
Resonant Freq. (GHz) Dielectric Constant
ε (at Resonant Freq.)
Quality Factor
Q(1/tanδ)
BST 11,377 0.0013 0.632 4423 133
BST-B 1,616 0.0095 1.417 1305 92
BST-C 7,370 0.0013 0.669 5817 298
BST-B-C 4,930 0.0058 0.813 3949 214
BST-CB6 4,240 0.0058 0.874 3415 251
930 8 12.8 3000 0.018 263
1000 4 13.5 4400 0.023 308
1077 0.005
x = 0.85 6.07 3.52 ± 0.77 1223 0.004
x = 0.95 5.95 4.86 ± 0.88 1288 0.005
x = 1.0 5.35 10.82 ± 0.53 1429 0.004
0.2wt% Li2O 7.8001 0.84 1307 0.024 322 27.16 7.21 53.7 401 76.6 86.3 4.63
0.3wt% Li2O 7.7806 0.49 1264 0.029 322 26.26 7.2 51.8 336 68.7 87.7 4.27
1310 300 0.0055 298 7.78
x=0.3 0.57 1393 341 0.0053 300 7.9
x=0.5 0.52 1150 305 0.0058 310 7.8
x=0.7 0.5 620 295 0.006 288 7.6
1080 x=0 0.48 1450 230 0.0061 7.57
x=0.1 0.41 1120 235 0.0061 7.58
x=0.15 0.47 1100 237 0.006 7.7
x=0.2 0.54 1150 305 0.0059 7.72
x=0.3 0.55 1200 325 0.0055 7.84
x=0.5 0.49 1000 310 0.0062 7.7
x=0.7 0.47 500 305 0.0068 7.57
1150 x=0 0.54 1690 280 0.0053 7.69
x=0.1 0.37 1300 230 0.0059 7.6
x=0.15 0.42 1000 200 0.0062 7.7
x=0.2 0.5 1100 290 0.006 7.8
x=0.3 0.52 1180 300 0.0058 7.65
x=0.5 0.47 1020 285 0.0068 7.5
x=0.7 0.43 500 280 0.0072
820 235 0.55 1618 0.0065 1052
850 235 0.55 1544 0.0067 1033
880 231 0.54 1454 0.0069 1030
1080 700 230 0.54 1238 0.0067 1005
750 235 0.55 1329 0.0064 1010
780 239 0.55 1356 0.0064 1048
800 241 0.55 1722 0.0063 1058
820 235 0.55 1617 0.0065 1047
850 232 0.54 1509 0.0065 1017
880 230 0.54 1379 0.007 1011
PZT: Fe 7.73 0.59 820 [5]
Pb0.9725(Zr0.52Ti0.48)0.945 7.8 0.591 1529 Our sample
측정불확도 측정불확도: 유전율, (측정장비: HP 4284A) : 2.32
측정불확도: tanδ, (측정장비: HP 4284A): 0.00026
▒ Influence of Bi2O3 and CuO addition on low-temperature sintering and dielectric properties of Ba0.6Sr0.4TiO3 ceramics의 참조표준 기본정보  
재료규격 - 조성: Ba0.6Sr0.4TiO3 + Glass Frit (Bi2O3, CuO, CuBi2O4)
- 시편형상 및 제조방법: Disk
- 원료순도: BaTiO3 (99.9%), SrTiO3 (99.9%), Bi2O3 (99.544%), CuO (98%)
- 혼합 및 분쇄: [BST] ball mill (24h), 미디어 ZrO2, 용매 에탄올 [CuBi2O4] ball mill (8h)
측정방법 - 측정/장비: 유전특성 LCR meter(HP 4284A), 고주파특성 N/W(HP 8753E)
- 시편형상: 재료규격 참조
- 소결특성: SEM 미세구조
- 측정환경: 유전특성 100Hz ~ 1MHz, 20oC
▒ Influence of Bi2O3 and CuO addition on low-temperature sintering and dielectric properties of Ba0.6Sr0.4TiO3 ceramics의 참조표준 문서자료  
  • [저널정보] Material Research Bulletin, in press / Influence of Bi2O3 and CuO addition on low-temperature sintering and dielectric properties of Ba0.6Sr0.4TiO3 ceramics / / / ( 2008)

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